7-溴-2H-[1,4]-苯并噻嗪-3(4H)-酮合成路线 (共 5 条)
反应条件
copper(l) iodide; trans-N,N'-dimethylcyclohexane-1,2-diamine; caesium carbonate in 1,4-dioxane T=100°C; Inert atmosphere;
参考文献
Huang, Wei-Sheng; Xu, Rongsong; Dodd, Rory; Shakespeare, William C.
Tetrahedron Letters, 2013 , vol. 54, # 38 p. 5214 - 5216
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide
参考文献
American Home Products Corporation; Ligand Pharmaceutical, Inc.
Patent: US6423699 B1, 2002 ;
反应条件
bromine; acetic acid T=50°C;
参考文献
Hanson, James R.; Richards, Lisa; Rozas, Panteleimon
Journal of Chemical Research, Miniprint, 2003 , # 11 p. 1120 - 1128
反应条件
triethylamine in methanol; water 0.333333 h; Heating;
参考文献
Sawhney, S N; Sharma, P. K.; Bajaj, K; Gupta, A
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 280 - 284
反应条件
1: H2O, CH3COONa / 0.5 h 2: 62 percent / Et3N / methanol; H2O / 0.33 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 33, p. 280 - 284