3-氯-4-甲酰基苯甲酸乙酯合成路线 （共 3 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=110°C; 2 h;
参考文献
Kelly, Michael G.; Kincaid, John; Duncton, Matthew; Sahasrabudhe, Kiran; Janagani, Satyanarayana; Upasani, Ravindra B.; Wu, Guoxian; Fang, Yunfeng; Wei, Zhi-Liang
Patent: US2006/194801 A1, 2006 ;
Location in patent: Page/Page column 45 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; carbon monoxide in N,N-dimethyl-formamide
T=110°C; 2 h;
参考文献
Zimmerman, Sommer S.; Khatri, Alpa; Garnier-Amblard, Ethel C.; Mullasseril, Praseeda; Kurtkaya, Natalie L.; Gyoneva, Stefka; Hansen, Kasper B.; Traynelis, Stephen F.; Liotta, Dennis C.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 6 p. 2334 - 2356
反应条件
1: methanol; tetrahydrofuran / 1 h / 0 - 20 °C
2: bis-triphenylphosphine-palladium(II) chloride; carbon monoxide / N,N-dimethyl-formamide / 2 h / 110 °C
View Scheme
参考文献
Zimmerman, Sommer S.; Khatri, Alpa; Garnier-Amblard, Ethel C.; Mullasseril, Praseeda; Kurtkaya, Natalie L.; Gyoneva, Stefka; Hansen, Kasper B.; Traynelis, Stephen F.; Liotta, Dennis C.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 6 p. 2334 - 2356
