4-(2-吡啶基)苯硼酸频哪醇酯合成路线 （共 3 条）
反应条件
1: 4-(pyrid-2-yl)bromobenzene With n-butyllithium in tetrahydrofuran T=-78°C; 1 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran
参考文献
AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH
Patent: WO2006/93466 A1, 2006 ;
Location in patent: Page/Page column 40 ;
反应条件
potassium acetate; tri-cyclo-hexyl-phosphine in 1,4-dioxane 20 h; Inert atmosphereReflux;
参考文献
BASF SE; BOERNER, Herbert Friedrich; LOEBL, Hans-Peter; SALBECK, Josef; POPOVA, Elena
Patent: US2013/231489 A1, 2013 ;
Location in patent: Paragraph 0184; 0185 ;
反应条件
1: methanol; water / 19 h / 23 °C 2: terpyridine; [(terpy)Pd(MeCN)][BF4]2; NAF; selectfluor / acetonitrile / 15 h / 23 °C View Scheme
参考文献
Mazzotti, Anthony R.; Campbell, Michael G.; Tang, Pingping; Murphy, Jennifer M.; Ritter, Tobias
Journal of the American Chemical Society, 2013 , vol. 135, # 38 p. 14012 - 14015
