乙基3-氨基-5-氰基-2-甲基异烟酸酯合成路线 （共 11 条）
反应条件
1: HNO3, / acetic anhydride
2: PCl3 / chlorobenzene
3: SnCl2, HCl
4: H2 / Pd/BaCO3
View Scheme
参考文献
Pieper; Yang; Zhou; Liu
Journal of the American Chemical Society, 1997 , vol. 119, # 8 p. 1809 - 1817
反应条件
1: PCl3 / chlorobenzene
2: SnCl2, HCl
3: H2 / Pd/BaCO3
View Scheme
参考文献
Pieper; Yang; Zhou; Liu
Journal of the American Chemical Society, 1997 , vol. 119, # 8 p. 1809 - 1817
反应条件
1: Et2NH
2: HNO3, / acetic anhydride
3: PCl3 / chlorobenzene
4: SnCl2, HCl
5: H2 / Pd/BaCO3
View Scheme
参考文献
Pieper; Yang; Zhou; Liu
Journal of the American Chemical Society, 1997 , vol. 119, # 8 p. 1809 - 1817
反应条件
palladium-barium carbonate; ethanol
P=760 Torr; Hydrogenation;
参考文献
Velluz; Amiard
Bulletin de la Societe Chimique de France, 1947 , p. 136,139
反应条件
Pd-BaSO4; ethanol
Hydrogenation;
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
Full Text Show Details
Ichiba; Emoto
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1941 , vol. 38, p. 347,350
反应条件
1: concentrated aqueous HCl
2: aqueous H2SO4; aqueous NaNO2 / 90 - 95 °C
3: ethanol / Erhitzen des vom Aethanol befreiten Reaktionsgemisches auf 115-125grad
4: lithium alanate; diethyl ether / 0 °C
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
反应条件
1: concentrated aqueous HCl
2: aqueous H2SO4; aqueous NaNO2 / 90 - 95 °C
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
Full Text Show Details
Ichiba; Emoto
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1941 , vol. 38, p. 347,350
反应条件
1: concentrated aqueous HCl
2: aqueous H2SO4; aqueous NaNO2 / 90 - 95 °C
3: diethyl ether; methanol / -15 °C
4: lithium alanate; diethyl ether / 0 °C
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
反应条件
hydrogenchloride; palladium on activated charcoal; acetic acid
Hydrogenation;
参考文献
Matsukawa; Shirakawa
Yakugaku Zasshi, 1951 , vol. 71, p. 1498
Chem.Abstr., 1952 , p. 8113
反应条件
ethanol; nickel
Hydrogenation;
参考文献
Velluz; Amiard
Bulletin de la Societe Chimique de France, 1947 , p. 136,139
