反应条件
1: 20 percent / 1.) pent-1-ynylcopper, hexamethylphosphoric triamide / diethyl ether / 1.) -20 deg C, room temperature, 1 h, 2.) -40 deg C, 10 min; -20 deg C, 30 min; 0 deg C, 1 h
2: 87 percent / m-chloroperbenzoic acid / CHCl3 / 1 h / -20 - -10 °C
View Scheme
参考文献
Batten, Richard J.; Coyle, John D.; Taylor, Richard J.K.; Vassiliou, Stamatios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1177 - 1182
