N,N-二甲基-1H-吲哚-5-磺酰胺合成路线 （共 5 条）
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 21 p. 3105 - 3109
反应条件
1: 56 percent / chlorosulfonic acid / 2 h / 70 °C
2: 64.2 percent / H2O; tetrahydrofuran / 30 - 35 °C
3: 47 percent / potassium permanganate / acetone; H2O / 2 h / 30 - 35 °C
4: 31.2 percent / 0.5 h / 238 - 240 °C
View Scheme
参考文献
Chachoyan, A. A.; Shkulev, V. A.; Samvelyan, K. G.; Garibdzhanyan, B. T.; Papayan, G. L.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 2 p. 126 - 129
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 2 p. 166 - 169
反应条件
1: 64.2 percent / H2O; tetrahydrofuran / 30 - 35 °C
2: 47 percent / potassium permanganate / acetone; H2O / 2 h / 30 - 35 °C
3: 31.2 percent / 0.5 h / 238 - 240 °C
View Scheme
参考文献
Chachoyan, A. A.; Shkulev, V. A.; Samvelyan, K. G.; Garibdzhanyan, B. T.; Papayan, G. L.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 2 p. 126 - 129
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 2 p. 166 - 169
反应条件
1: 47 percent / potassium permanganate / acetone; H2O / 2 h / 30 - 35 °C
2: 31.2 percent / 0.5 h / 238 - 240 °C
View Scheme
参考文献
Chachoyan, A. A.; Shkulev, V. A.; Samvelyan, K. G.; Garibdzhanyan, B. T.; Papayan, G. L.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 2 p. 126 - 129
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 2 p. 166 - 169
反应条件
T=238 - 240°C; 0.5 h;
参考文献
Chachoyan, A. A.; Shkulev, V. A.; Samvelyan, K. G.; Garibdzhanyan, B. T.; Papayan, G. L.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 2 p. 126 - 129
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 2 p. 166 - 169
