4-[[[(4-甲基苯基)磺酰基]氧基]甲基]-2,6-吡啶二甲酸2,6-二甲酯合成路线 （共 4 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1.5 h;
参考文献
Tang, Rui-ren; Zhao, Qiang; Yan, Zi-er; Luo, Yi-ming
Synthetic Communications, 2006 , vol. 36, # 14 p. 2027 - 2034
反应条件
1: 41 percent / FeSO4*7H20; H2O2; H2SO4 / H2O / 15 - 30 °C 2: 81 percent / triethylamine / CH2Cl2 / 1.5 h / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 36, # 14 p. 2027 - 2034
反应条件
1: CH3COCl 2: 41 percent / FeSO4*7H20; H2O2; H2SO4 / H2O / 15 - 30 °C 3: 81 percent / triethylamine / CH2Cl2 / 1.5 h / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 36, # 14 p. 2027 - 2034
反应条件
lithium bromide in acetone T=20°C; 2 h;
参考文献
Su, Xun-Cheng; Man, Bradley; Beeren, Sophie; Liang, Haobo; Simonsen, Shane; Schmitz, Christophe; Huber, Thomas; Messerle, Barbara A.; Otting, Gottfried
Journal of the American Chemical Society, 2008 , vol. 130, # 32 p. 10486 - 10487
