N,N’-二[(S)-1-(叔-丁基二甲基硅烷基氧基甲基)丙基]草酸二酰胺合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 24 h; Heating;
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
pyridine in dichloromethane
T=0 - 25°C;
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr
2: 100 percent / pyridine / CH2Cl2 / 0 - 25 °C
View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 88 percent / hydrogen; triethylamine / Pd/C / methanol / 12 h / 760 Torr
2: 95 percent / pyridine / 0 - 25 °C
3: 75 percent / sodium azide / dimethylformamide / 30 h / 60 °C
4: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr
5: 100 percent / pyridine / CH2Cl2 / 0 - 25 °C
View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 75 percent / sodium azide / dimethylformamide / 30 h / 60 °C
2: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr
3: 100 percent / pyridine / CH2Cl2 / 0 - 25 °C
View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
反应条件
1: 95 percent / pyridine / 0 - 25 °C
2: 75 percent / sodium azide / dimethylformamide / 30 h / 60 °C
3: 95 percent / hydrogen; triethylamine / Pd/C / methanol / 6 h / 760 Torr
4: 100 percent / pyridine / CH2Cl2 / 0 - 25 °C
View Scheme
参考文献
Kotkar, Shriram P.; Sudalai, Arumugam
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1738 - 1742
