1.1: bis(benzonitrile)palladium(II) dichloride / toluene / 1.75 h / Inert atmosphere; Reflux 2.1: ammonia; sodium / tetrahydrofuran / 0.42 h / -78 °C 2.2: 0.08 h View Scheme
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Quilez Del Moral, Jose F.; Arteaga, Pilar; Meine, Niklas; Perez-Morales, M. Carmen; Catalan, Julieta V.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 4 p. 1118 - 1125
1.1: bis(benzonitrile)palladium(II) dichloride / toluene / 1.75 h / Inert atmosphere; Reflux 2.1: ammonia; sodium / tetrahydrofuran / 0.42 h / -78 °C 2.2: 0.08 h View Scheme
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Quilez Del Moral, Jose F.; Arteaga, Pilar; Meine, Niklas; Perez-Morales, M. Carmen; Catalan, Julieta V.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 4 p. 1118 - 1125
borane-THF; (S)-Corey-Bakshi-Shibata reagent in tetrahydrofuran; toluene
Cooling with iceInert atmosphere;
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Quilez Del Moral, Jose F.; Arteaga, Pilar; Meine, Niklas; Perez-Morales, M. Carmen; Catalan, Julieta V.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 4 p. 1118 - 1125
