反应条件
1: ethanol / 144 h / 20 °C / Reflux 2: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3: water; N,N-dimethyl-formamide / 90 °C 4: sulfuric acid / 2 h / 90 °C 5: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Morley, Andrew; Tomkinson, Nicholas; Cook, Andrew; MacDonald, Catherine; Weaver, Richard; King, Sarah; Jenkinson, Lesley; Unitt, John; McCrae, Christopher; Phillips, Tim
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 20 p. 6031 - 6035