2-羟基-5-甲基间苯二甲醇合成路线 (共 49 条)
反应条件
methanesulfonic acid in tetrahydrofuran
参考文献
Khaniani, Yeganeh; Golchoubian, Hamid
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 12 p. 2817 - 2823
参考文献
NOVOMER, INC.; Allen, Scott D.; Cherian, Anna E.; Simoneau, Chris A.; Farmer, Jay J.; Coates, Geoffrey W.; Gridnev, Alexei; LaPointe, Robert E.
Patent: US2013/144032 A1, 2013 ;
Location in patent: Paragraph 0368 ;
反应条件
1: 95 percent / conc. H2SO4 / acetone / 1 h / 20 °C 2: 95 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / 20 °C 3: 90 percent / conc. HCl / 12 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 24 p. 8297 - 8300
反应条件
1: glacial acetic acid; HCl 2: concentrated sulfuric acid View Scheme
参考文献
Fries; Brandes
Justus Liebigs Annalen der Chemie, 1939 , vol. 542, p. 48,63
参考文献
Zawadowski,T.
Roczniki Chemii, 1968 , vol. 42, p. 297 - 307
反应条件
1,4-dioxane; copper oxide-chromium oxide T=175°C; Hydrogenation;
参考文献
Fries; Brandes
Justus Liebigs Annalen der Chemie, 1939 , vol. 542, p. 48,63
反应条件
copper oxide-chromium oxide T=200°C; P=128714 Torr; Hydrogenolyse;
参考文献
Connor; Adkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 4680
反应条件
1,4-dioxane; copper oxide-chromium oxide Hydrogenolyse;
参考文献
Kennedy
Chemistry and Industry (London, United Kingdom), 1940 , p. 297
参考文献
Barclay; Burawoy; Thomson
Journal of the Chemical Society, 1944 , p. 400,403
反应条件
dimethyl selenoxide in benzene 2 h; Heating;
参考文献
Syper; Mlochowski
Synthesis, 1984 , vol. NO. 9, p. 747 - 752