2-羟基-5-甲基间苯二甲醇合成路线 （共 49 条）
反应条件
1: 94 percent / HCl / 12 h
2: 78 percent / NaOMe / 12 h
3: PhI(OAc)2 / CH2Cl2 / 2.5 h / 20 °C
4: 52 percent / Dess Martin periodinane / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Liu, Qin; Rovis, Tomislav
Journal of the American Chemical Society, 2006 , vol. 128, # 8 p. 2552 - 2553
参考文献
Sartori, Giovanni; Bigi, Franca; Maggi, Raimondo; Porta, Cecilia
Tetrahedron Letters, 1994 , vol. 35, # 38 p. 7073 - 7076
反应条件
1: 94 percent / HCl / 12 h
2: 78 percent / NaOMe / 12 h
3: PhI(OAc)2 / CH2Cl2 / 2.5 h / 20 °C
View Scheme
参考文献
Liu, Qin; Rovis, Tomislav
Journal of the American Chemical Society, 2006 , vol. 128, # 8 p. 2552 - 2553
反应条件
hydrogenchloride in dichloromethane
T=20°C; 24 h;
参考文献
Chirakul; Hampton; Bencze
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8297 - 8300
反应条件
1: NaOH
2: 100 percent / PBr3
View Scheme
参考文献
Lin, Cai-Xia; Kong, Xiao-Fei; Li, Qing-Shan; Zhang, Zheng-Zhi; Yuan, Yao-Feng; Xu, Feng-Bo
CrystEngComm, 2013 , vol. 15, # 35 p. 6948 - 6962
参考文献
Arnaud, Nathalie; Picard, Claude; Cazaux, Louis; Tisnes, Pierre
Tetrahedron, 1997 , vol. 53, # 40 p. 13757 - 13768
反应条件
potassium carbonate in acetone
12 h; Heating;
参考文献
Kato-Toma, Yoko; Imajo, Seiichi; Ishiguro, Masaji
Tetrahedron Letters, 1998 , vol. 39, # 1-2 p. 51 - 54
参考文献
Arcoleo; Oliverio
Ricerca Scientifica, 1954 , vol. 24, p. 62,65
参考文献
Ullmann; Brittner
Chemische Berichte, 1909 , vol. 42, p. 2546
