1-溴-2,4,6-三乙基苯合成路线 (共 5 条)
反应条件
magnesium 1.) THF; 2.) 1 h, RT; 2 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 120, p. 1331 - 1338
反应条件
bromine; iron in tetrachloromethane
参考文献
Clayden, Jonathan; Pink, Jennifer H.; Westlund, Neil; Frampton, Christopher S.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 7 p. 901 - 917
反应条件
1: AlCl3
2: tetrachloromethane; bromine / 0 °C / Lichtausschluss
View Scheme
参考文献
Nauta; Mulder
Recueil des Travaux Chimiques des Pays-Bas, 1939 , vol. 58, p. 514,517
反应条件
bromine; iron
T=0 - 20°C; Bromination;
参考文献
Kolotuchin, Sergei V.; Thiessen, Paul A.; Fenlon, Edward E.; Wilson, Scott R.; Loweth, Colin J.; Zimmerman, Steven C.
Chemistry - A European Journal, 1999 , vol. 5, # 9 p. 2537 - 2547
反应条件
magnesium in diethyl ether
参考文献
Clayden, Jonathan; Darbyshire, Megan; Pink, Jennifer H.; Westlund, Neil; Wilson, Francis X.
Tetrahedron Letters, 1997 , vol. 38, # 49 p. 8587 - 8590