1,1'-联(2,4-环戊二烯-1-亚基)合成路线 (共 26 条)
反应条件
in benzene
byproducts: t-BuOH; Irradiation (UV/VIS); digermane soln. irradiating in the presence of an excess of t-Bu2O2 for30 min; product content detd. by high-pressure chromy.;
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
反应条件
in benzene
byproducts: t-BuOH; Irradiation (UV/VIS); digermane soln. irradiating in the presence of an excess of t-Bu2O2 for1 h; product content detd. by high-pressure chromy.;
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
反应条件
in benzene
byproducts: t-BuOH; Irradiation (UV/VIS); trigermane soln. irradiating in the presence of an excess of t-Bu2O2 for 1 h; product content detd. by high-pressure chromy.;
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
反应条件
in benzene Irradiation (UV/VIS); irradiating for 3 h in the presence of an excess of disulfide; detd. by high-pressure chromy.;
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
反应条件
phosphorus pentoxide in xylene
2 h; Heating;
参考文献
Griffith; Gentile; Robichaud; Frankenheim
Journal of medicinal chemistry, 1984 , vol. 27, # 8 p. 995 - 1003
反应条件
1: 122.0 g / Et3N / CHCl3 / 2 h / Ambient temperature
2: 88.1 g / P2O5 / xylene / 2 h / Heating
View Scheme
参考文献
Griffith; Gentile; Robichaud; Frankenheim
Journal of medicinal chemistry, 1984 , vol. 27, # 8 p. 995 - 1003