in quinoline under exclusion of water; mixt. of phthalonitrile, anhyd. InCl3 and distd. deoxygenated quinoline refluxed for 1 h; cooled to ca. 273 K; filtered; washed with toluene and MeOH; dried at 383 K; elem. anal.;
(Ar); stirring at -78°C, heating at reflux temp. for 15 min.; product dissolved in sulfuric acid and precipitated with ice-water mixture;
参考文献
Diaz-Garcia, Maria A.; Agullo-Lopez, Fernando; Sastre, Angela; Torres, Tomas; Torruellas, William E.; Stegeman, George I.
Journal of Physical Chemistry, 1995 , vol. 99, # 41 p. 14988 - 14991
