反应条件
in not given from phthalonitrile and 4-tert-butylphthalonitrile using the usual template react. technique (Moser and Thomas, Phthalocyanines, CRC Press, Florida (1983), Vol.II, Chap.1); refluxing with acetone after react. (2 h), filtration from insol. ZnPc (washing with acetone and 5percentaq. HCl for prepn.), washing (several times, hot acetone), evapn. of filtrate to dryness, purifn. (chromy. on silica, diethylether as eluent); elem. anal.;
参考文献
Konami, Hideo; Hatano, Masahiro
Chemistry Letters, 1988 , # 9 p. 1359 - 1362
