potassium hydroxide in dimethyl sulfoxide
T=189.85°C; 0.166667 h; microwave irradiation;
参考文献
Diaz-Ortiz, Angel; Elguero, Jose; Foces-Foces, Concepcion; De La Hoz, Antonio; Moreno, Andres; Del Carmen Mateo, Maria; Sanchez-Migallon, Ana; Valiente, Gema
New Journal of Chemistry, 2004 , vol. 28, # 8 p. 952 - 958
in ethylene glycol dimethyl ether
dehydrating a MnCl2*4H2O soln. by boiling for 1 h, addn. of phthalodinitrile, boiling for 1 h; pptn., filtration, washing with water and acetone, drying in vac. over KOH, elem. anal.;
参考文献
Grunewald, Horst; Homborg, Heiner
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 4 p. 483 - 489