反应条件
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 3 h, 2.) THF, hexane, from -60 deg C to RT, 3 h 2: 97 percent / H2, 85percent aq. phosphoric acid / 5percent Pd/C / ethanol / 6 h / 60 °C / 2280 Torr 3: 96 percent / 48percent aq. HBr, acetic acid / 4 h / Heating View Scheme
参考文献
Majetich; Liu
Synthetic Communications, 1993 , vol. 23, # 16 p. 2331 - 2335
