反应条件
1: 2.5 M n-butyllithium / diethyl ether; hexane / 48 h / Ambient temperature 2: 1.) p-toluenesulfonyl azide; 2.) tetrabutylammonium hydrogen sulfate, sodium borohydride / 1.) ether, -78 deg C, 5 h; 2.) water, rt to 30 deg C View Scheme
参考文献
Kelly, T. Ross; Maguire, Martin P.
Tetrahedron, 1985 , vol. 41, # 15 p. 3033 - 3036