反应条件
1: 1.) n-BuLi, 2.) I2 / 1.) THF, hexane, from -10 deg C to RT, 2 h, 2.) THF, 20 deg C, 2 h
2: 50 percent / Pd(OAc)2, n-Bu4NCl, KOAc, PPh3 / dimethylformamide / 72 h / 80 °C
3: 65 percent / trimethylsilyl iodide / CHCl3 / 1 h / Ambient temperature
View Scheme
参考文献
Essamkaoui; Mayrargue; Vierfond; Reynet; Moskowitz; Thal
Synthetic Communications, 1992 , vol. 22, # 18 p. 2723 - 2728
