in water byproducts: CO, H2; React. of starting materials at room temp. (N2 or Ar).; Evolution of gas (CO, H2) obsd. (gas chromy.). Extn. (Et2O) of resulting red soln., drying (vac.) of collected ether ext. Addn. of a second equiv of (H-Quin)Cl dissolved in H2O to the extd. mixt. causes vigorous evolution of CO and H2. IR spectroscopy.;
in water byproducts: CO, H2; React. of starting materials at room temp. (N2 or Ar).; Evolution of gas (CO, H2) obsd. (gas chromy.). Extn. (Et2O) of resulting red soln., drying (vac.) of collected ether ext. Addn. of a second equiv of (H-Quin)Cl dissolved in H2O to the extd. mixt. causes vigorous evolution of CO and H2. IR spectroscopy.;
