2,4-二甲氧基苯甲酸合成路线 （共 127 条）
反应条件
sodium hydroxide; dihydrogen peroxide in methanol; water 20 h; Ambient temperature;
参考文献
Ferrari, F.; Lima, R. Alves De; Bettolo, G. B. Marini
Phytochemistry (Elsevier), 1984 , vol. 23, # 11 p. 2691 - 2692
反应条件
potassium hydroxide in ethanol 24 h; Heating;
参考文献
Phytochemistry (Elsevier), , vol. 28, # 6 p. 1778 - 1779
反应条件
1: 50 mg / K2CO3 / acetone / 50 h / Heating 2: 30 mg / 40percent KOH aq. / ethanol / 24 h / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 28, # 6 p. 1778 - 1779
反应条件
manganese triacetate in acetic acid 0.0166667 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 2 p. 545 - 550
反应条件
sodium hydroxide in methanol 72 h; other reag.; other solvent; Product distribution;
参考文献
Arai, Eri; Tokuyama, Hidetoshi; Linsell, Martin S.; Fukuyama, Tohru
Tetrahedron Letters, 1998 , vol. 39, # 1-2 p. 71 - 74
反应条件
2: 9 percent / manganese(III) acetate / acetic acid / 0.02 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 2 p. 545 - 550
反应条件
1: MgSO4 / CH2Cl2 / 2 h / 0 - 5 °C 2: 1.) triethylamine (1.2 to 1.5 molar equiv.) / CH2Cl2 / Ambient temperature 3: methylhydrazine / CH2Cl2 / 1.) 2 h, r.t; 2.) 8 h, 35 deg C; 3.) r.t 4: propylene oxide / CH2Cl2 / 1.5 h / Ambient temperature 5: 68 mg / >1.6 molar equiv. K2S2O8, K2HPO4 / acetonitrile; H2O / 2 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 7 p. 2646 - 2659
反应条件
1: 1.) triethylamine (1.2 to 1.5 molar equiv.) / CH2Cl2 / Ambient temperature 2: methylhydrazine / CH2Cl2 / 1.) 2 h, r.t; 2.) 8 h, 35 deg C; 3.) r.t 3: propylene oxide / CH2Cl2 / 1.5 h / Ambient temperature 4: 68 mg / >1.6 molar equiv. K2S2O8, K2HPO4 / acetonitrile; H2O / 2 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 7 p. 2646 - 2659
反应条件
1: propylene oxide / CH2Cl2 / 1.5 h / Ambient temperature 2: 68 mg / >1.6 molar equiv. K2S2O8, K2HPO4 / acetonitrile; H2O / 2 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 7 p. 2646 - 2659
反应条件
1: methylhydrazine / CH2Cl2 / 1.) 2 h, r.t; 2.) 8 h, 35 deg C; 3.) r.t 2: propylene oxide / CH2Cl2 / 1.5 h / Ambient temperature 3: 68 mg / >1.6 molar equiv. K2S2O8, K2HPO4 / acetonitrile; H2O / 2 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 7 p. 2646 - 2659
