反应条件
1.1: potassium hydroxide / water / 0.67 h / 50 °C / |Inert atmosphere; |Large scale
1.2: 5 h / 50 °C / |Inert atmosphere; |Large scale
2.1: boron trifluoride diethyl etherate / tetrahydrofuran / 15 h / 20 - 25 °C / |Inert atmosphere; |Large scale
2.2: 3 h / 20 - 38 °C / |Inert atmosphere; |Large scale
2.3: 0.5 h / 5 - 30 °C / |Inert atmosphere; |Large scale
View Scheme
参考文献
Wang, Youchu; Papamichelakis, Maria; Chew, Warren; Sellstedt, John; Noureldin, Razzak; Tadayon, Sam; Daigneault, Sylvain; Galante, Rocco J.; Sun, Jerry
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1253 - 1260