1.1: 98 percent / H2; TFA / 10percent Pd/C / 60 h / 20 °C 2.1: 79 percent / Ac2O / 120 h / 150 - 160 °C 3.1: O3 / CH2Cl2; methanol / -77 °C 3.2: 89 percent / Me2S / CH2Cl2; methanol / -77 - 20 °C 4.1: 88 percent / 30percent aq. H2O2; HCO2H / 3 h / 20 °C View Scheme
参考文献
Bell, Thomas W.; Khasanov, Alisher B.; Drew, Michael G. B.; Filikov, Anton; James, Thomas L.
Angewandte Chemie - International Edition, 1999 , vol. 38, # 17 p. 2543 - 2547
1.1: 98 percent / H2; TFA / 10percent Pd/C / 60 h / 20 °C 2.1: 79 percent / Ac2O / 120 h / 150 - 160 °C 3.1: O3 / CH2Cl2; methanol / -77 °C 3.2: 89 percent / Me2S / CH2Cl2; methanol / -77 - 20 °C View Scheme
参考文献
Bell, Thomas W.; Khasanov, Alisher B.; Drew, Michael G. B.; Filikov, Anton; James, Thomas L.
Angewandte Chemie - International Edition, 1999 , vol. 38, # 17 p. 2543 - 2547
