3-羟基-N,N-二乙基苯胺合成路线 （共 78 条）
反应条件
in toluene 2 h; Reflux;
参考文献
Elsinghorst, Paul W.; Haertig, Wolfgang; Goldhammer, Simone; Grosche, Jens; Guetschow, Michael
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 19 p. 3940 - 3946
反应条件
in toluene 2 h; Heating;
参考文献
Knierzinger; Wolfbeis
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 2 p. 225 - 229
反应条件
1: N,N-diethyl-m-aminophenol With hydrogenchloride; sodium nitrite in water T=0 - 5°C; 4 h; 2: α-naphthol in N,N-dimethyl-formamide T=70°C; 8 h;
参考文献
Ionescu, Andreea; Godbert, Nicolas; Crispini, Alessandra; Termine, Roberto; Golemme, Attilio; Ghedini, Mauro
Journal of Materials Chemistry, 2012 , vol. 22, # 44 p. 23617 - 23626
反应条件
trichlorophosphate T=90 - 100°C; 3 h;
参考文献
Kirpichenok, M. A.; Gorozhankin, S. K.; Grandberg, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 6 p. 693 - 697
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 6 p. 830 - 835
反应条件
1: 40 percent / POCl3 / 3 h / 90 - 100 °C 2: 27 percent / hydrazine hydrate / dimethylformamide / 0.5 h / Ambient temperature View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 6 p. 693 - 697
Khimiya Geterotsiklicheskikh Soedinenii, , # 6 p. 830 - 835
参考文献
Hoechst Aktiengesellschaft
Patent: US4160764 A1, 1979 ;
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate T=0°C; 3.5 h; 2: N,N-diethyl-m-aminophenol T=0 - 95°C; 9 h;
参考文献
Dalapati, Sasanka; Jana, Sankar; Guchhait, Nikhil
Chemistry Letters, 2011 , vol. 40, # 3 p. 279 - 281
反应条件
sodium hydroxide; sodium carbonate
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3027
