3-羟基-N,N-二乙基苯胺合成路线 （共 78 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=50°C; 48 h; Inert atmosphere;
参考文献
Karaoglu, H.R. Pekbelgin; Koca, Atf; Kocak, Makbule Burkut
Dyes and Pigments, 2012 , vol. 92, # 3 p. 1005 - 1017
反应条件
1: N,N-diethyl-m-aminophenol With hydrogenchloride; sodium nitrite in water
T=0 - 5°C; 4 h;
2: 1,7-dihydroxy-naphthalene in N,N-dimethyl-formamide
T=70°C; 8 h;
参考文献
Ionescu, Andreea; Godbert, Nicolas; Crispini, Alessandra; Termine, Roberto; Golemme, Attilio; Ghedini, Mauro
Journal of Materials Chemistry, 2012 , vol. 22, # 44 p. 23617 - 23626
反应条件
zinc(II) chloride in ethanol
Heating;
参考文献
Kalmykova, E. A.; Kuznetsova, N. A.; Kaliya, O. L.; Tavrizova, M. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 4.2. p. 1003 - 1010,911 - 916
反应条件
1: 2-amino-quinoline With sodium amide in ethanol
5 h; Heating;
2: With isopentyl nitrite in ethanol
0.5 h; Heating;
3: N,N-diethyl-m-aminophenol With carbon dioxide in ethanol
48 h;
参考文献
Yang, Ya-Ling; Miao, Ming-Ming; Lin, Qiang; Yang, Guang-Yu
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 1 p. 19 - 24
反应条件
1: triethylamine / benzene / 3 h / 20 °C
2: benzene / 0.5 h / Heating
3: 94 percent / water / dimethylsulfoxide / 24 h / 20 °C
View Scheme
参考文献
Vovk; Bol'but; Lebed'; Boiko
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 1 p. 101 - 105
反应条件
1.1: trichlorophosphate / 5 - 10 °C
1.2: 4 h / 5 - 75 °C
1.3: Cooling with ice
2.1: phosphorus trichoride / ethanol / 4 h / 40 - 60 °C
2.2: 20 °C / pH 8
View Scheme
参考文献
Padalkar, Vikas S.; Tathe, Abhinav; Gupta, Vinod D.; Patil, Vikas S.; Phatangare, Kiran; Sekar
Journal of Fluorescence, 2012 , vol. 22, # 1 p. 311 - 322
参考文献
Mitsubishi Chem. Ind.
Patent: CH616654DE2545389 , 19801976 ;
Chem.Abstr., 1976 , vol. 85, # 108434
反应条件
1: 82 percent / triethylamine / tetrahydrofuran / 1 h
2: 34 percent / benzene / 12 h / Heating
View Scheme
参考文献
Haworth; Lamberton; Woodcock
Journal of the Chemical Society, 1947 , p. 179
反应条件
1: With hydrogenchloride in water; isopropyl alcohol
T=20°C; 3.66667 h;
2: With ammonium hydrogen carbonate in water; isopropyl alcohol
1.58333 h;
参考文献
WISTA LABORATORIES LTD.; CLUNAS, Scott; STRORY, John, Mervyn, David; RICKARD, Janet, Elizabeth; HORSLEY, David; HARRINGTON, Charles, Robert; WISCHIK, Claude, Michel
Patent: WO2010/67078 A2, 2010 ;
Location in patent: Page/Page column 64, 65 ;
反应条件
hydrogenchloride; sodium acetate
参考文献
Biehringer
Journal fuer Praktische Chemie (Leipzig), 1896 , vol. <2> 54, p. 235
Full Text Show Details
Leonhardt and Co.
Patent: DE63081 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 93
Full Text Show Details
Leonhardt and Co.
Patent: DE58955 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 92
