3-羟基-N,N-二乙基苯胺合成路线 （共 78 条）
参考文献
Biehringer
Journal fuer Praktische Chemie (Leipzig), 1896 , vol. <2> 54, p. 235
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Leonhardt and Co.
Patent: DE58995 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 92,93
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Leonhardt and Co.
Patent: DE63081 ;
反应条件
potassium carbonate in acetone
12 h; Reflux;
参考文献
Yao, Wei; Huang, Dejian
Organic Letters, 2010 , vol. 12, # 4 p. 736 - 738
反应条件
hydrogenchloride; sodium nitrite in water
T=0°C; 3 h;
参考文献
Lee, Haekyung; Choi, Myung Gil; Yu, Hyo-Yeon; Ahn, Sangdoo; Chang, Suk-Kyu
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 12 p. 3539 - 3542
反应条件
hydrogenchloride; sodium nitrite in water
T=0 - 5°C; 4 h;
参考文献
Ionescu, Andreea; Godbert, Nicolas; Crispini, Alessandra; Termine, Roberto; Golemme, Attilio; Ghedini, Mauro
Journal of Materials Chemistry, 2012 , vol. 22, # 44 p. 23617 - 23626
参考文献
Moehlau
Chemische Berichte, 1892 , vol. 25, p. 1065
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B.A.S.F.
Patent: DE45268 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 2, p. 174
反应条件
1.1: trichlorophosphate / 5 - 10 °C
1.2: 4 h / 5 - 75 °C
1.3: Cooling with ice
2.1: phosphorus trichoride / ethanol / 4 h / 40 - 60 °C
2.2: 20 °C / pH 8
View Scheme
参考文献
Padalkar, Vikas S.; Tathe, Abhinav; Gupta, Vinod D.; Patil, Vikas S.; Phatangare, Kiran; Sekar
Journal of Fluorescence, 2012 , vol. 22, # 1 p. 311 - 322
反应条件
1: 2-amino-benzothiazole With sulfuric acid; acetic acid; sodium nitrite in water
T=-5°C;
2: N,N-diethyl-m-aminophenol in methanol; water
T=0 - 5°C; 2.5 h;
参考文献
Tao, Tao; Xu, Feng; Chen, Xiao-Chun; Liu, Qian-Qian; Huang, Wei; You, Xiao-Zeng
Dyes and Pigments, 2012 , vol. 92, # 3 p. 916 - 922
反应条件
1: diethyl ether / 1 h
2: aq. ethanol / 6 h / Heating
View Scheme
参考文献
Il'chenko, A. Ya.; Koval'chuk, R. E.; Krokhtyak, V. I.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 2348 - 2349
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 12 p. 2630 - 2631
