(Z)-4-乙氧基-1,1,1-三氟-3-丁烯-2-酮合成路线 （共 3 条）
反应条件
hydraziniumdihydrochloride in ethanol 6 h; Heating / reflux;
参考文献
REDDY US THERAPEUTICS, INC.; PAL, Manojit; KHANNA, Ish; SUBRAMANIAN, Venkataraman; PADAKANTI, Srinivas; PILLARISETTI, Sivaram
Patent: WO2006/58201 A2, 2006 ;
Location in patent: Page/Page column 132 ;
反应条件
pyridine in dichloromethane
T=20°C; 18 h;
参考文献
Chopin, Nicolas; Medebielle, Maurice; Pilet, Guillaume
Journal of Fluorine Chemistry, 2013 , vol. 155, p. 89 - 96
反应条件
T=80°C; 1.33333 h; Inert atmosphere; Product distribution / selectivity;
参考文献
SOLVAY SA; BRAUN, Max; PALSHERM, Stefan; CLAASSEN, Uta
Patent: WO2011/3854 A1, 2011 ;
Location in patent: Page/Page column 16 ;
