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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
91028-07-8
合成路线
（共 8 条）
91028-07-8
→
反应条件
10557-20-7
+
1122-91-4
4-溴苯甲醛
反应条件
silver tetrafluoroborate; PPh3 gold(I) chloro complex; sulfuric acid; water in 1,4-dioxane T=60°C; 24 h;
参考文献
Cui, Dong-Mei; Zhuang, Dan-Wen; Chen, Ying; Zhang, Chen
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 860 - 865
589-87-7
对溴碘苯
→
反应条件
91028-07-8
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide; triethylamine; 1,2-bis(diphenylphosphino)-ortho-carborane in acetonitrile T=80 - 100°C; 48 h;
参考文献
Nakamura, Hiroyuki; Kamakura, Takaya; Onagi, Shinya
Organic Letters, 2006 , vol. 8, # 10 p. 2095 - 2098
589-87-7
对溴碘苯
+
53915-69-8
1,2-丙二烯三正丁基锡
→
反应条件
91028-07-8
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in N,N-dimethyl-formamide T=25°C; 12 h;
参考文献
Huang, Chih-Wei; Shanmugasundaram, Muthian; Chang, Hao-Ming; Cheng, Chien-Hong
Tetrahedron, 2003 , vol. 59, # 20 p. 3635 - 3641
2039-82-9
4-溴苯乙烯
+
75-25-2
三溴甲烷
→
反应条件
91028-07-8
反应条件
1: With Et3NBnCl; sodium hydroxide in dichloromethane; water T=0 - 20°C; Doering-LaFlamme allene synthesis; Inert atmosphere; 2: With ethyl magnesium chloride in tetrahydrofuran T=0°C; Doering-LaFlamme allene synthesis; 2 h; Inert atmosphere;
参考文献
Yonehara, Mitsuhiro; Nakamura, Shinji; Muranaka, Atsuya; Uchiyama, Masanobu
Chemistry - An Asian Journal, 2010 , vol. 5, # 3 p. 452 - 455
1228107-76-3
→
反应条件
91028-07-8
反应条件
[XPhosAu(NCCH3)]SbF6 in chloroform T=60°C;
参考文献
Bolte, Benoit; Odabachian, Yann; Gagosz, Fabien
Journal of the American Chemical Society, 2010 , vol. 132, # 21 p. 7294 - 7296
51884-07-2
→
反应条件
91028-07-8
反应条件
chromium hexacarbonyl in dimethyl sulfoxide T=130°C; Inert atmosphere;
参考文献
Lin, Shaw-Tao; Lee, Chuan-Chen; Ding, Mei-Fang; Liang, David W.; Jeng, An-Ting
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 529 - 534
589-87-7
对溴碘苯
+
106-96-7
3-溴丙炔
→
反应条件
91028-07-8
反应条件
1: 4-bromo-1-iodobenzene With tBu4ZnLi2 in tetrahydrofuran T=0°C; Inert atmosphere; 2: propargyl bromide in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Furayama, Taniyuki; Yonehara, Mitsuhiro; Arimoto, Sho; Kobayashi, Minoru; Matsumoto, Yotaro; Uchiyama, Masanobu
Chemistry - A European Journal, 2008 , vol. 14, # 33 p. 10348 - 10356
→
反应条件
91028-07-8
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium methylate in N,N-dimethyl-formamide T=20°C; Suzuki-Miyaura cross coupling reaction; 3 h; Inert atmosphere;
参考文献
Radkowski, Karin; Seidel, Guenter; Fuerstner, Alois
Chemistry Letters, 2011 , vol. 40, # 9 p. 950 - 952
