Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Basavaiah, Deevi; Kulkarni, Surendra U.; Bhat, Narayan G.; Prasad, J. V. N. Vara
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 239 - 246
1,1'-bis-(diphenylphosphino)ferrocene; potassium hydroxide; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in ethylene glycol dimethyl ether T=80°C; 16 h; Title compound not separated from byproducts;
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Basavaiah, Deevi; Kulkarni, Surendra U.; Bhat, Narayan G.; Prasad, J. V. N. Vara
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 239 - 246
methanesulfonic acid in tetrahydrofuran
dropwise addn. of CH3Li (1 equiv.) to soln. of C6H11B(OC3H6O) (2.5 mmol) in THF at -78°C via syringe; stirring at -78°C for 3 h; addn. of CH3SO3H at -78/25°C; warming slowly to room temp.; stirring at room temp.;; not isolated; product distribution (depending on temp. at which acid is added) is determined by 11B-NMR;;
参考文献
Brown, Herbert C.; Vasumathi, Nagarajan; Joshi, Navalkishore N.
Organometallics, 1993 , vol. 12, p. 1058 - 1067
