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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
91111-41-0
合成路线
（共 10 条）
91111-41-0
→
反应条件
773-99-9
2-(1-萘基)乙醇
反应条件
1: 97 percent / acetic anhydride / Heating 2: 86 percent / sulphur / 4 h / 200 - 220 °C 3: 84 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Mitra, Ashutosh; Ghoshe, Swati
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 8 p. 785 - 789
91111-41-0
→
反应条件
13686-49-2
1-(2-溴乙基)萘
反应条件
1: 97 percent / acetic anhydride / Heating 2: 86 percent / sulphur / 4 h / 200 - 220 °C 3: 84 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / Heating 4: 55 percent / phosphorus tribromide / benzene / Heating View Scheme
参考文献
Mitra, Ashutosh; Ghoshe, Swati
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 8 p. 785 - 789
91111-41-0
→
反应条件
2122-70-5
alpha-萘乙酸乙酯
反应条件
1: 97 percent / acetic anhydride / Heating 2: 86 percent / sulphur / 4 h / 200 - 220 °C View Scheme
参考文献
Mitra, Ashutosh; Ghoshe, Swati
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 8 p. 785 - 789
91111-41-0
→
反应条件
4725-34-2
反应条件
1: aq. HCl / tetrahydrofuran / 2 h / 20 °C 2: 88 percent / LiAlH4 / tetrahydrofuran / 2.5 h / 0 - 20 °C View Scheme
参考文献
Ferraz, Helena M.C; Silva Jr., Luiz F
Tetrahedron, 2001 , vol. 57, # 50 p. 9939 - 9949
91111-41-0
→
反应条件
62677-71-8
1,2,3,4-四氢萘-1-乙酸乙酯
+
54125-45-0
反应条件
phosphorus pentoxide in benzene 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Miyashi,T.; Nishizawa,Y.; Fujii,Y.
Journal of the American Chemical Society, 1986 , vol. 108, p. 1617
91111-41-0
→
反应条件
62741-60-0
反应条件
sulfuric acid; hydrogen; palladium on activated charcoal 1.) toluene, reflux, 2.) EtOH; Yield given. Multistep reaction;
参考文献
Perez; Angel; Charris; Torres; Israel
Bollettino chimico farmaceutico, 1995 , vol. 134, # 6 p. 329 - 332
91111-41-0
→
反应条件
54125-45-0
反应条件
acetic anhydride Heating;
参考文献
Mitra, Ashutosh; Ghoshe, Swati
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 8 p. 785 - 789
91111-41-0
→
反应条件
62677-71-8
1,2,3,4-四氢萘-1-乙酸乙酯
+
54125-45-0
反应条件
phosphorus pentoxide in benzene 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Miyashi,T.; Nishizawa,Y.; Fujii,Y.
Journal of the American Chemical Society, 1986 , vol. 108, p. 1617
91111-41-0
→
反应条件
54125-45-0
+
94834-50-1
反应条件
hydrogenchloride in tetrahydrofuran T=20°C; 2 h;
参考文献
Ferraz, Helena M.C; Silva Jr., Luiz F
Tetrahedron, 2001 , vol. 57, # 50 p. 9939 - 9949
91111-41-0
→
反应条件
54125-45-0
+
94834-49-8
反应条件
sulfuric acid in toluene Heating; Title compound not separated from byproducts;
参考文献
Perez; Angel; Charris; Torres; Israel
Bollettino chimico farmaceutico, 1995 , vol. 134, # 6 p. 329 - 332
