1: With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.75 h;
2: With tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-78 - -20°C;
3: With hydrogenchloride; water in tetrahydrofuran; hexane
参考文献
SPEEDEL EXPERIMENTA AG
Patent: WO2006/103273 A1, 2006 ;
Location in patent: Page/Page column 42 ;
WO 2006/103273 A1