1,3-二(二异丙基膦酰)丙烷合成路线 (共 3 条)
反应条件
in diethyl ether; hexane
ice cooling then Rt, 10 h;
参考文献
Tani, Kazuhide; Tanigawa, Eiji; Tatsuno, Yoshitaka; Otsuka, Sei
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 87 - 102
反应条件
in tetrahydrofuran
T=20°C; Grignard reaction; 3 h;
参考文献
Lindner, Ekkehard; Schmid, Markus; Wald, Joachim; Queisser, Joachim A.; Gepraegs, Michael; Wegner, Peter; Nachtigal, Christiane
Journal of Organometallic Chemistry, 2000 , vol. 602, # 1-2 p. 173 - 187
反应条件
1: diethyl ether
2: diethyl ether
View Scheme
参考文献
Campora; Lopez; Maya; Palma; Carmona; Valerga
Journal of Organometalic Chemistry, 2002 , vol. 643-644, p. 331 - 341