N-(1-金刚烷酰氧基)吡啶-2-硫酮合成路线 (共 42 条)
反应条件
sulfur; sodium tetrahydroborate 1) CH2Cl2, irradiation, 0 deg C, 1 h, 2) MeOH, CH2Cl2, RT, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Castagnino, Enzo; Jaszberenyi, Joseph Cs.
Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6057 - 6060
反应条件
1: 33 percent Spectr. / CH2Cl2 / 0 - 5 °C / Irradiation 2: aq.K2CO3 / acetone / 12 h / 25 °C View Scheme
参考文献
Barton, Derek H. R.; Chern, Ching-Yuh; Jaszberenyi, Joseph Cs.
Tetrahedron Letters, 1992 , vol. 33, # 35 p. 5013 - 5016
反应条件
Sb(SPh)3 in diethyl ether 1 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Bridon, Dominique; Zard, Samir Z.
Journal of the Chemical Society, Chemical Communications, 1985 , # 16 p. 1066 - 1068
反应条件
oxygen in pyridine; acetic acid 2 h; Ambient temperatureIrradiationvarious oxygen pressure; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 18 p. 7144 - 7149
反应条件
1,1-dichloro-2,2-difluoroethylene in acetonitrile 6 h; Irradiation;
参考文献
Tetrahedron, , vol. 51, # 7 p. 1903 - 1920
反应条件
sulfur in dichloromethane T=0°C; 1 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 33 p. 6057 - 6060
反应条件
in dichloromethane 0.5 h; Ambient temperatureIrradiation; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 53, # 36 p. 12067 - 12088
反应条件
sulfur T=120°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 33 p. 6057 - 6060
反应条件
in acetonitrile 6 h; Irradiation;
参考文献
Tetrahedron, , vol. 51, # 7 p. 1903 - 1920
反应条件
9-borabicyclo[3.3.1]nonane dimer; tri-n-butyl-tin hydride in toluene T=0°C;
参考文献
Perchyonok, V. Tamara; Schiesser, Carl H.
Tetrahedron Letters, 1998 , vol. 39, # 30 p. 5437 - 5438