N-(1-金刚烷酰氧基)吡啶-2-硫酮合成路线 (共 42 条)
反应条件
1: 1-hydroxy-2(1H)-pyridinethione With sodium hydride in acetonitrile
Red light;
2: adamantane-1-carbonyl chloride in acetonitrile
Red light;
参考文献
Jankowiak, Aleksandra; Kaszynski, Piotr
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7441 - 7448
反应条件
1: oxalyl chloride, dimethyl formamide / benzene / 2 h / Ambient temperature
2: CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Barton, Derek H.R.; Bridon, Dominique; Zard, Samir Z.
Heterocycles, 1987 , vol. 25, p. 449 - 462
反应条件
tributylphosphine in dichloromethane
0.5 h; Ambient temperature;
参考文献
Barton; Samadi
Tetrahedron, 1992 , vol. 48, # 35 p. 7083 - 7090
反应条件
in dichloromethane
Ambient temperature;
参考文献
Barton, Derek H. R.; Bridon, Dominique; Fernandez-Picot, Isabel; Zard, Samir Z.
Tetrahedron, 1987 , vol. 43, # 12 p. 2733 - 2740
反应条件
in dichloromethane
T=-60°C; Irradiation;
参考文献
Barton, Derek H. R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.; Reibenspies
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8050 - 8059
反应条件
in dichloromethane
168 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
Title/Abstract View citing articles Show Details
Barton, Derek H. R.; Ferreira, J. Albert
Phosphorus, Sulfur and Silicon and Related Elements, 1997 , vol. 120-121, p. 1 - 20
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
in dichloromethane
Ambient temperatureIrradiation;
参考文献
Barton, Derek H. R.; Garcia, Begona; Togo, Hideo; Zard, Samir Z.
Tetrahedron Letters, 1986 , vol. 27, # 12 p. 1327 - 1330
反应条件
oxygen in pyridine; acetic acid
2 h; Ambient temperatureIrradiationvarious oxygen pressure; Product distribution;
参考文献
Barton, Derek H. R.; Halley, Frank; Ozbalik, Nubar; Schmitt, Martine; Young, Esme; Balavoine, Gilbert
Journal of the American Chemical Society, 1989 , vol. 111, # 18 p. 7144 - 7149
反应条件
2-trimethylsilanyloxy-acrylic acid ethyl ester in dichloromethane
T=0 - 5°C; Irradiation;
参考文献
Barton, Derek H. R.; Chern, Ching-Yuh; Jaszberenyi, Joseph Cs.
Tetrahedron, 1995 , vol. 51, # 7 p. 1867 - 1886