N-(1-金刚烷酰氧基)吡啶-2-硫酮合成路线 (共 42 条)
反应条件
3-phenyl-3-(trifluoromethyl)-3H-diazirine in dichloromethane
T=0 - 5°C; Irradiation;
参考文献
Barton, Derek H.R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.
Journal of the American Chemical Society, 1992 , vol. 114, # 14 p. 5904 - 5905
反应条件
benzenesulphonyl azide in dichloromethane
T=5°C; 4 h; Sunlight irradiation;
参考文献
Nyfeler, Erich; Renaud, Philippe
Organic Letters, 2008 , vol. 10, # 5 p. 985 - 988
反应条件
in dichloromethane
T=0 - 5°C; Irradiation;
参考文献
Barton, Derek H.R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.
Journal of the American Chemical Society, 1992 , vol. 114, # 14 p. 5904 - 5905
反应条件
1,1-dichloro-2,2-difluoroethylene in acetonitrile
6 h; Irradiation;
参考文献
Okano, Takashi; Takakura, Nobuyuki; Nakano, Yuko; Okajima, Asako; Eguchi, Shoji
Tetrahedron, 1995 , vol. 51, # 7 p. 1903 - 1920
反应条件
sulfur in dichloromethane
T=0°C; 1 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Barton, Derek H. R.; Castagnino, Enzo; Jaszberenyi, Joseph Cs.
Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6057 - 6060
反应条件
in acetonitrile
Ambient temperatureIrradiation;
参考文献
Okano; Takakura; Nakano; Eguchi
Tetrahedron Letters, 1992 , vol. 33, # 24 p. 3491 - 3494
反应条件
in dichloromethane; benzene
Ambient temperatureIrradiationduring work up excess monomer was destroyed by hydrazine;
参考文献
Barton, Derek H. R.; Togo, Hideo; Zard, Samir Z.
Tetrahedron Letters, 1985 , vol. 26, # 51 p. 6349 - 6352
反应条件
in dichloromethane
0.5 h; Ambient temperatureIrradiation; Yields of byproduct given;
参考文献
Barton, Derek H. R.; Liu, Wansheng
Tetrahedron, 1997 , vol. 53, # 36 p. 12067 - 12088
反应条件
in dichloromethane
Ambient temperatureIrradiation;
参考文献
Barton, Derek H. R.; Garcia, Begona; Togo, Hideo; Zard, Samir Z.
Tetrahedron Letters, 1986 , vol. 27, # 12 p. 1327 - 1330
反应条件
sulfur
T=120°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Barton, Derek H. R.; Castagnino, Enzo; Jaszberenyi, Joseph Cs.
Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6057 - 6060