(2S)-5-氧代-1,2-吡咯烷二羧酸二叔丁酯合成路线 (共 7 条)
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate 2 h; Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 34, # 9 p. 3873 - 3878
反应条件
1: 95 percent / RuO2 hydrate, 10percent aqueous NaIO4 / ethyl acetate / 2 h / Ambient temperature 2: 90 percent / CF3COOH / CH2Cl2 / 0.33 h / Ambient temperature 3: diethyl ether; methanol / 0.5 h / 0 °C View Scheme
参考文献
Yoshifuji,Shigeyuki; Tanaka, Ken-ichi; Kawai, Tomoyuki; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3873 - 3878
反应条件
1: 95 percent / RuO2 hydrate, 10percent aqueous NaIO4 / ethyl acetate / 2 h / Ambient temperature 2: 90 percent / CF3COOH / CH2Cl2 / 0.33 h / Ambient temperature View Scheme
参考文献
Yoshifuji,Shigeyuki; Tanaka, Ken-ichi; Kawai, Tomoyuki; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3873 - 3878
反应条件
hydrogenchloride in water T=20°C; 2 h;
参考文献
Barraclough, Paul; Spray, Caroline A.; Young, Douglas W.
Tetrahedron Letters, 2005 , vol. 46, # 27 p. 4653 - 4655
反应条件
tin(II) trifluoromethanesulfonate in dichloromethane T=20°C; 2 h;
参考文献
Bose, D. Subhas; Kumar, K. Kiran; Reddy, A.V. Narsimha
Synthetic Communications, 2003 , vol. 33, # 3 p. 445 - 450
反应条件
hydrogenchloride in ethyl acetate Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 11 p. 3216 - 3218
反应条件
water; iodine in acetonitrile 5 h; Heating;
参考文献
Yadav; Balanarsaiah; Raghavendra; Satyanarayana
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4921 - 4924