5-异丙基异恶唑-3-甲酸乙酯合成路线 （共 3 条）
反应条件
hydroxylamine hydrochloride in ethanol T=15 - 25°C; 1 h; Heating / reflux;
参考文献
Piotrowski, David W.; Rogers, Bruce N.; McWhorter JR., William W.; Walker, Daniel Patrick; Corbett, Jeffrey W.; Groppi JR., Vincent E.; Rudmann, Daniel G.
Patent: US2003/236287 A1, 2003 ;
Location in patent: Page 45, 46 ;
US 20030236287 A1
反应条件
1: 81 percent / NaH / toluene / 1 h / Heating 2: 76 percent / NH2OH*HCl / ethanol / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 47 p. 7509 - 7512
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 34, # 47 p. 7509 - 7512
