1-苄基嘧啶-2,4,6(1h,3h,5h)-三酮合成路线 （共 11 条）
反应条件
sodium methylate in methanol 12 h; Reflux;
参考文献
Jurok, Radek; Cibulka, Radek; Dvorakova, Hana; Hampl, Frantisek; Hodacova, Jana
European Journal of Organic Chemistry, 2010 , # 27 p. 5217 - 5224
反应条件
hydrogenchloride in ethanol, diethylmalonate; ethanol; water
参考文献
US2003/78276 A1, ;
US 20030078276 A1
反应条件
hydrogenchloride in ethanol 0.833333 h; Heating;
参考文献
Krasnov, K. A.; Slesarev, V. I.; Selimanova, I. N.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 7 p. 1215 - 1220
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 7 p. 1531 - 1537
反应条件
acetic anhydride; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 71, p. 390
反应条件
1: 42 percent / NaOCH3 / dimethylsulfoxide; methanol / 0.5 h / 60 - 70 °C 2: 83 percent / conc. aq. HCl / ethanol / 0.83 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 7 p. 1215 - 1220
Zhurnal Organicheskoi Khimii, , vol. 28, # 7 p. 1531 - 1537
反应条件
1: 55 percent / benzene / 1.) 60 min, reflux; 12 h, room temp. 2: 2.) H2O / 1.) dioxane, 30 min View Scheme
参考文献
, vol. 1984, # 6 p. 1193 - 1204
反应条件
water 1.) dioxane, 30 min; Yield given. Multistep reaction;
参考文献
, vol. 1984, # 6 p. 1193 - 1204
参考文献
Chemische Berichte, , vol. 15, p. 2842
Justus Liebigs Annalen der Chemie, , vol. 222, p. 250
反应条件
trichlorophosphate in water 2 h; Heating;
参考文献
Nagamatsu, Tomohisa; Yamasaki, Hirofumi; Yoneda, Fumio
Heterocycles, 1994 , vol. 37, # 2 p. 1147 - 1164
反应条件
1: 32 percent / POCl3 / H2O / 2 h / Heating
2: 71 percent / 25percent aq. NH3, Zn / ethanol / 4 h / 90 °C
View Scheme
参考文献
Nagamatsu, Tomohisa; Yamasaki, Hirofumi; Yoneda, Fumio
Heterocycles, 1994 , vol. 37, # 2 p. 1147 - 1164
