1-(6-苄氧基-2,2-二甲基-3a,4,6,6a-四氢呋喃并[3,4-d][1,3]二氧杂环戊烯-4-基)-2-三苯甲基氧基-乙酮合成路线 （共 6 条）
反应条件
acetic anhydride
T=25°C; 16 h;
参考文献
Legler, Guenter; Juelich, Elisabeth
Carbohydrate Research, 1984 , vol. 128, p. 61 - 72
反应条件
acetic anhydride; dimethyl sulfoxide
T=25°C; 16 h;
参考文献
Legler, Guenter; Juelich, Elisabeth
Carbohydrate Research, 1984 , vol. 128, p. 61 - 72
反应条件
1: 94 percent / 12M HCl / methanol; H2O / 7 h / Ambient temperature
2: 66 g / pyridine / 18 h / 25 °C
3: 65 percent / acetic anhydride / 16 h / 25 °C
View Scheme
参考文献
Legler, Guenter; Juelich, Elisabeth
Carbohydrate Research, 1984 , vol. 128, p. 61 - 72
反应条件
1: 66 g / pyridine / 18 h / 25 °C
2: 65 percent / acetic anhydride / 16 h / 25 °C
View Scheme
参考文献
Legler, Guenter; Juelich, Elisabeth
Carbohydrate Research, 1984 , vol. 128, p. 61 - 72
反应条件
1: 78 percent / methyltri-n-octylammonium chloride, 10M NaOH / benzene / 30 h / Ambient temperature
2: 94 percent / 12M HCl / methanol; H2O / 7 h / Ambient temperature
3: 66 g / pyridine / 18 h / 25 °C
4: 65 percent / acetic anhydride / 16 h / 25 °C
View Scheme
参考文献
Legler, Guenter; Juelich, Elisabeth
Carbohydrate Research, 1984 , vol. 128, p. 61 - 72
反应条件
1: 78 percent / methyltri-n-octylammonium chloride, 10M NaOH / benzene / 30 h / Ambient temperature
2: 94 percent / 12M HCl / methanol; H2O / 7 h / Ambient temperature
3: 66 g / pyridine / 18 h / 25 °C
4: 65 percent / acetic anhydride / 16 h / 25 °C
View Scheme
参考文献
Legler, Guenter; Juelich, Elisabeth
Carbohydrate Research, 1984 , vol. 128, p. 61 - 72
