1-乙炔基-6,6-二甲基环己烯合成路线 （共 3 条）
反应条件
trichlorophosphate in pyridine
T=100°C; 2 h;
参考文献
Gartner; Oesterhelt; Seifer-Schiller; et al.
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5654 - 5659
反应条件
Yield given. Multistep reaction;
参考文献
Stuetz, Anton; Granitzer, Waltraud; Roth, Sabine
Tetrahedron, 1985 , vol. 41, # 23 p. 5685 - 5696
反应条件
1: 1.) sodium amide / 1.) diethyl ether, reflux, 30 min; 2.) reflux, 1 h
2: 85 percent / sodium amide, Fe(NO3)3 / diethyl ether / 2.33 h
3: 45 percent / POCl3 / pyridine / 2 h / 100 °C
View Scheme
参考文献
Gartner; Oesterhelt; Seifer-Schiller; et al.
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5654 - 5659
