1-二苯甲基-3-苯基氮杂丁烷合成路线 （共 4 条）
反应条件
hydrogen; palladium(II) hydroxide/carbon in ethanol T=20°C; P=3000.3 Torr; 20.25 h;
参考文献
Briner, Karin; Camp, Anne Marie; Cornell, Alan; Mazanetz, Michael Philip; Rothhaar, Roger Ryan; Victor, Frantz; Williams, Andrew Caerwyn; Zhang, Deyi
Patent: US2008/214520 A1, 2008 ;
Location in patent: Page/Page column 21 ;
反应条件
copper(I) bromide in tetrahydrofuran; diethyl ether
T=20 - 50°C; 17.5 h;
参考文献
Briner, Karin; Camp, Anne Marie; Cornell, Alan; Mazanetz, Michael Philip; Rothhaar, Roger Ryan; Victor, Frantz; Williams, Andrew Caerwyn; Zhang, Deyi
Patent: US2008/214520 A1, 2008 ;
Location in patent: Page/Page column 21 ;
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile
T=70°C;
参考文献
Hillier, Michael C.; Chen, Cheng-Yi
Journal of Organic Chemistry, 2006 , vol. 71, # 20 p. 7885 - 7887
反应条件
1: ethyldiisopropylamine / acetonitrile / -20 - -10 °C
2: ethyldiisopropylamine / acetonitrile / 70 °C
View Scheme
参考文献
Hillier, Michael C.; Chen, Cheng-Yi
Journal of Organic Chemistry, 2006 , vol. 71, # 20 p. 7885 - 7887
