反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere
3.1: potassium hydrogen persulfate; 18-crown-6 ether; sodium hydrogencarbonate; acetone / water; acetonitrile / 0 °C / Inert atmosphere
4.1: benzene / UV-irradiation; Inert atmosphere
View Scheme
参考文献
Shao, Yutian; Yang, Chao; Gui, Weijun; Liu, Yang; Xia, Wujiong
Chemical Communications, 2012 , vol. 48, # 29 p. 3560 - 3562