反应条件
1.1: tetrahydrofuran / 0 °C
2.1: pyridinium chlorochromate / dichloromethane / 20 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 °C
3.2: 6 h / 0 °C
3.3: 8 h
4.1: copper(II) bis(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 1 h / 82 °C / |Inert atmosphere
View Scheme
参考文献
Liu, Wei-Min; Tnay, Ya Lin; Gan, Kian Ping; Liu, Zhen-Hong; Tyan, Wan Huei; Narasaka, Koichi
Helvetica Chimica Acta, 2012 , vol. 95, # 10 p. 1953 - 1969,17
Title/Abstract Full Text Show Details
Liu, Wei-Min; Tnay, Ya Lin; Gan, Kian Ping; Liu, Zhen-Hong; Tyan, Wan Huei; Narasaka, Koichi
Helvetica Chimica Acta, 2012 , vol. 95, # 10 p. 1953 - 1969
