4-异硫氰酸-1,5-二甲基-2-苯基-1,2-二氢吡唑-3-酮合成路线 （共 7 条）
反应条件
0.166667 h; Irradiationmicrowave;
参考文献
Li, Jianping; Ma, Chunming; Qu, Guirong
Heteroatom Chemistry, 2006 , vol. 17, # 2 p. 148 - 151
反应条件
sodium hydrogencarbonate in chloroform; water
pH=7 - 7.5;
参考文献
Gelder, Joel M. Van; Klein, Joseph Y.; Basel, Yochai; Reizelman, Anat; Tchilibon, Susanna; Mouallem, Orly
Patent: US2008/39456 A1, 2008 ;
Location in patent: Page/Page column 53 ;
反应条件
1: With triethylamine in benzene
T=70 - 80°C; 3 h;
2: With chloroformic acid ethyl ester; triethylamine in chloroform
T=20°C; 1 h;
参考文献
Ma, Chun-Ming; Li, Jian-Ping; Zheng, Peng-Zhi
Heterocycles, 2005 , vol. 65, # 2 p. 359 - 364
反应条件
ammonia; benzene
und Behandeln des Reaktionsprodukts mit COCl2 in Benzol;
参考文献
Farbw.Hoechst
Patent: DE951721 , 1952 ;
参考文献
Takahashi; Kanematsu
Yakugaku Zasshi, 1959 , vol. 79, p. 172,175
Chem.Abstr., 1959 , p. 13138
参考文献
Takahashi; Kanematsu
Yakugaku Zasshi, 1959 , vol. 79, p. 172,175
Chem.Abstr., 1959 , p. 13138
反应条件
0.25 h; Irradiationmicrowave;
参考文献
Li, Jianping; Ma, Chunming; Qu, Guirong
Heteroatom Chemistry, 2006 , vol. 17, # 2 p. 148 - 151
