bromine; triphenylphosphine in acetonitrile
T=20°C; Substitution; 24 h;
参考文献
Cabezon, Beatriz; Cao, Jianguo; Raymo, Francisco M.; Stoddart, J. Fraser; White, Andrew J. P.; Williams, David J.
Chemistry - A European Journal, 2000 , vol. 6, # 12 p. 2262 - 2273
1: 90 percent / LiAlH4 / tetrahydrofuran / 24 h / 20 °C
2: 67 percent / Br2; Ph3P / acetonitrile / 24 h / 20 °C
View Scheme
参考文献
Cabezon, Beatriz; Cao, Jianguo; Raymo, Francisco M.; Stoddart, J. Fraser; White, Andrew J. P.; Williams, David J.
Chemistry - A European Journal, 2000 , vol. 6, # 12 p. 2262 - 2273
1: 43 percent / K2CO3 / acetonitrile / 24 h / 60 °C
2: 90 percent / LiAlH4 / tetrahydrofuran / 24 h / 20 °C
3: 67 percent / Br2; Ph3P / acetonitrile / 24 h / 20 °C
View Scheme
参考文献
Cabezon, Beatriz; Cao, Jianguo; Raymo, Francisco M.; Stoddart, J. Fraser; White, Andrew J. P.; Williams, David J.
Chemistry - A European Journal, 2000 , vol. 6, # 12 p. 2262 - 2273