反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '605303', constants.ctx, '0')">acetyl chloride</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11323438', constants.ctx, '0')">AlCl<sub>3</sub>, aluminium chloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0°C; Friedel-Crafts acylation; 0.166667 h; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1906415', constants.ctx, '0')">monoiodonaphthalene</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0 - 20°C; Friedel-Crafts acylation; 120 h; Inert atmosphere; <br /> <br />
参考文献
Wiley, Jenny L.; Smith, Valerie J.; Chen, Jianhong; Martin, Billy R.; Huffman, John W. Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 6 p. 2067 - 2081