1: With zinc(II) chloride in dichloromethane T=23°C; Mukaiyama aldol-lactonization; 60 h; Inert atmosphere; 2: With hydrogen fluoride in acetonitrile T=0 - 23°C; Inert atmosphere; optical yield given as percent de;
参考文献
Richardson, Robyn D.; Knowles, Lynn M.; Cieplak, Piotr; Smith, Jeffrey W.; Ma, Gil; Oyola, Yatsandra; Zancanella, Manuel; Romo, Daniel
Journal of Medicinal Chemistry, 2008 , vol. 51, # 17 p. 5285 - 5296
1: With zinc(II) chloride in dichloromethane T=23°C; Mukaiyama aldol-lactonization; 60 h; Inert atmosphere; 2: With hydrogen fluoride in acetonitrile T=0 - 23°C; Inert atmosphere; optical yield given as percent de;
参考文献
Richardson, Robyn D.; Knowles, Lynn M.; Cieplak, Piotr; Smith, Jeffrey W.; Ma, Gil; Oyola, Yatsandra; Zancanella, Manuel; Romo, Daniel
Journal of Medicinal Chemistry, 2008 , vol. 51, # 17 p. 5285 - 5296
