2-(4-甲氧基苯基)哌嗪合成路线 (共 3 条)
反应条件
1: in tetrahydrofuran; methanol T=0°C; 0.166667 h; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol T=0°C;
参考文献
MITSUBISHI PHARMA CORPORATION; SANOFI-SYNTHELABO
Patent: WO2004/85408 A1, 2004 ;
Location in patent: Page 262-263 ;
WO 2004/085408 A1
反应条件
palladium on activated charcoal; hydrogen in methanol 4 h;
参考文献
Kour, Harpreet; Paul, Satya; Singh, Parvinder Pal; Gupta, Monika; Gupta, Rajive
Tetrahedron Letters, 2013 , vol. 54, # 8 p. 761 - 764
反应条件
1: HgO*2HBF4 / tetrahydrofuran / 6 h / 70 °C / |Inert atmosphere 2: palladium on activated charcoal; hydrogen / methanol / 4 h View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 8 p. 761 - 764