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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
91528-99-3
合成路线
（共 8 条）
91528-99-3
+
672-66-2
二甲基苯基磷
→
反应条件
反应条件
diethyl ether in dichloromethane under Ar for 1h; concentrated by removal of solvent in vacuo; diethyl ether added; solid collected;; IR; GC-MS;;
参考文献
Perrier, S.; Kochi, J.K.
Inorganic Chemistry, 1988 , vol. 27, p. 4165 - 4173
91528-99-3
+
110-83-8
环己烯
→
反应条件
930-68-7
2-环己烯-1-酮
+
1561-86-0
2-氯环己醇
+
286-20-4
环氧环己烷
+
822-87-7
2-氯环己酮
反应条件
in acetonitrile cyclohexene in decane was added to a solution of (Ph4P)O2RuCl3; several hours; diethyl ether added;; GC-MS; MS;;
参考文献
Inorganic Chemistry, , vol. 27, p. 4165 - 4173
91528-99-3
+
128-39-2
2,6-二叔丁基苯酚
→
反应条件
719-22-2
2,6-二叔丁基苯醌
+
2455-14-3
3,3',5,5'-四叔丁基-4,4'-联苯醌
反应条件
in acetonitrile after 2 h solvent was mostly removed in vacuo; addn. of diethyl ether;; (1)H-NMR;;
参考文献
Perrier, S.; Kochi, J.K.
Inorganic Chemistry, 1988 , vol. 27, p. 4165 - 4173
91528-99-3
+
128-39-2
2,6-二叔丁基苯酚
→
反应条件
719-22-2
2,6-二叔丁基苯醌
+
2455-14-3
3,3',5,5'-四叔丁基-4,4'-联苯醌
反应条件
in acetonitrile after 2 h solvent was mostly removed in vacuo; addn. of diethyl ether;; (1)H-NMR;;
参考文献
Inorganic Chemistry, , vol. 27, p. 4165 - 4173
91528-99-3
+
110-83-8
环己烯
→
反应条件
930-68-7
2-环己烯-1-酮
+
1561-86-0
2-氯环己醇
+
286-20-4
环氧环己烷
+
822-87-7
2-氯环己酮
反应条件
in acetonitrile cyclohexene in decane was added to a solution of (Ph4P)O2RuCl3; several hours; diethyl ether added;; GC-MS; MS;;
参考文献
Perrier, S.; Kochi, J.K.
Inorganic Chemistry, 1988 , vol. 27, p. 4165 - 4173
91528-99-3
+
110-83-8
环己烯
→
反应条件
930-68-7
2-环己烯-1-酮
+
1561-86-0
2-氯环己醇
+
286-20-4
环氧环己烷
+
822-87-7
2-氯环己酮
反应条件
in acetonitrile cyclohexene in decane was added to a solution of (Ph4P)O2RuCl3; several hours; diethyl ether added;; GC-MS; MS;;
参考文献
Perrier, S.; Kochi, J.K.
Inorganic Chemistry, 1988 , vol. 27, p. 4165 - 4173
91528-99-3
+
110-83-8
环己烯
→
反应条件
930-68-7
2-环己烯-1-酮
+
1561-86-0
2-氯环己醇
+
286-20-4
环氧环己烷
+
822-87-7
2-氯环己酮
反应条件
in acetonitrile cyclohexene in decane was added to a solution of (Ph4P)O2RuCl3; several hours; diethyl ether added;; GC-MS; MS;;
参考文献
Perrier, S.; Kochi, J.K.
Inorganic Chemistry, 1988 , vol. 27, p. 4165 - 4173
91528-99-3
→
反应条件
反应条件
triphenylphosphine in acetonitrile stirred for 3 h; concentrated by removal of solvent in vacuo; diethyl ether added; solid collected;; filtrate analysed by GC-MS;;
参考文献
Perrier, S.; Kochi, J.K.
Inorganic Chemistry, 1988 , vol. 27, p. 4165 - 4173
